Methyl iodide → HCID 19075278, 화합물

HRID 727325노트

반응식

HRID 727325 반응식
[CH3:1][I:2].[CH2:3]([O:9][C:10]1[C:11]([C:15]2[CH:16]=[N:17][CH:18]=[CH:19][CH:20]=2)=[N:12][S:13][N:14]=1)[CH2:4]/[CH:5]=[CH:6]/[CH2:7][CH3:8]>CC(C)=O>[I-:2].[CH2:3]([O:9][C:10]1[C:11]([C:15]2[CH:16]=[N+:17]([CH3:1])[CH:18]=[CH:19][CH:20]=2)=[N:12][S:13][N:14]=1)[CH2:4]/[CH:5]=[CH:6]/[CH2:7][CH3:8]

참가 물질

4

반응물 2

HCID 6328Methyl iodideHCID 19075284HCID 19075284, 화합물

생성물 1

HCID 19075278HCID 19075278, 화합물

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

A mixture of methyl iodide (1 ml, 15 mmol) and trans-3-(4-(3- hexenyloxy)-1,2,5-thiadiazol-3-yl)pyridine (3 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.90 g (75%).

후처리

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.90 g (75%)

출처 및 근거

ORD 기록
ord-a87d3aa81b374279a5dfd2a8b2153468
출처 데이터셋
uspto-grants-1998_01
특허 번호
US05712297

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