Methyl iodide → 3-(3-(2-(2-Butoxyethoxy) ethoxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide

HRID 727346

반응식

HRID 727346 반응식
[CH3:1][I:2].[CH2:3]([O:7][CH2:8][CH2:9][O:10][CH2:11][CH2:12][O:13][C:14]1[C:15]([C:19]2[CH:20]=[N:21][CH:22]=[CH:23][CH:24]=2)=[N:16][S:17][N:18]=1)[CH2:4][CH2:5][CH3:6]>CC(C)=O>[I-:2].[CH2:3]([O:7][CH2:8][CH2:9][O:10][CH2:11][CH2:12][O:13][C:14]1[C:15]([C:19]2[CH:20]=[N+:21]([CH3:1])[CH:22]=[CH:23][CH:24]=2)=[N:16][S:17][N:18]=1)[CH2:4][CH2:5][CH3:6]

참가 물질

4

반응물 2

HCID 6328Methyl iodideHCID 190753243-(3-(2-(2-Butoxyethoxy)ethoxy)-1,2,5-thiadiazol-4-yl)pyridine

생성물 1

HCID 190752543-(3-(2-(2-Butoxyethoxy) ethoxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

A mixture of methyl iodide (0.5 ml, 9 mmol) and 3-(4-(2-(2-butoxyethoxy)ethoxy)-1,2,5-thiadiazol-3-yl)pyridine (3 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration.

후처리

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration

출처 및 근거

ORD 기록
ord-5f1363628b3f44bfa56e4a3e8531ffe7
출처 데이터셋
uspto-grants-1998_01
특허 번호
US05712297

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