Ammonia → HCID 178429957, 화합물

HRID 729194

반응식

HRID 729194 반응식
[NH2:1][C:2]1[C:3](=[O:15])[N:4]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[N:5]([CH3:8])[C:6]=1[CH3:7].[Cl:16][C:17]1[CH:18]=[C:19]([OH:23])[CH:20]=[CH:21][CH:22]=1.N>O.CC(O)C.[Fe-3](C#N)(C#N)(C#N)(C#N)(C#N)C#N.[K+].[K+].[K+]>[Cl:16][C:17]1/[C:22](=[N:1]/[C:2]2[C:3](=[O:15])[N:4]([C:9]3[CH:10]=[CH:11][CH:12]=[CH:13][CH:14]=3)[N:5]([CH3:8])[C:6]=2[CH3:7])/[CH:21]=[CH:20][C:19](=[O:23])[CH:18]=1

참가 물질

7

반응물 3

HCID 222AmmoniaHCID 21514-AminoantipyrineHCID 79333-Chlorophenol

생성물 1

HCID 178429957HCID 178429957, 화합물

시약·촉매·용매 3

HCID 178511488HCID 178511488, 화합물촉매HCID 962Water용매HCID 3776Isopropanol용매

실험 절차

10 mmol of 4-amino-1,5-dimethyl-2-phenyl-1,2-dihydro-3H-pyrazol-3-one was dissolved in 30 ml of water. This solution was admixed with 10 mmol of 3-chlorophenol in solution in 30 ml of 2-propanol, 3 ml of 20% aqueous ammonia and 22 mmol of potassium ferricyanide at a temperature ranging from 5 to 10° C.

후처리

  1. customranging from 5 to 10° C.

출처 및 근거

ORD 기록
ord-90d47fe86fee49e6960a89f297290853
출처 데이터셋
uspto-grants-2009_09
특허 번호
US07582123B2

연결된 노트

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