4-Bromoanisole → 4-Methoxy-4'-methyldiphenylamine

HRID 737249

반응식

HRID 737249 반응식
COc1ccc(Br)cc1.Cc1ccc(N)cc1>CC(C)c1cc(C(C)C)c(-c2ccccc2[P](C2CCCCC2)(C2CCCCC2)->[Pd]2(<-[NH2]c3ccccc3-c3cccc[c]32)[O]S(=O)(=O)C(F)(F)F)c(C(C)C)c1.CN1CCCN2CCCN=C12.CS(C)=O>COc1ccc(Nc2ccc(C)cc2)cc1

참가 물질

6

반응물 2

HCID 77304-BromoanisoleHCID 7813p-Toluidine

생성물 1

HCID 114358284-Methoxy-4'-methyldiphenylamine수율 11.111%

시약·촉매·용매 3

HCID 1235837-Methyl-1,5,7-triazabicyclo[4.4.0]dec-5-ene시약HCID 178439018HCID 178439018, 화합물촉매HCID 679Dimethyl Sulfoxide용매5회

반응 조건

온도
60 °C

실험 절차

These solutions were added to a 384- well source plate (80 µL per well). The Mosquito HTS liquid handling robot was used to dose each of these solutions (200 nL each) into a 1536-well plate.

후처리

  1. addition기록된 절차가 없습니다

출처 및 근거

ORD 기록
ord-c0c49ddf3b4b48808b0d66ba314e280a
출처 데이터셋
Ahneman

연결된 노트

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