Hydrochloric Acid → HCID 19427131, 화합물

HRID 741788

반응식

HRID 741788 반응식
[CH2:1]([Si:9](Cl)(Cl)Cl)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH3:13][O:14][CH2:15][CH2:16][O:17][CH2:18][CH2:19][OH:20].Cl>CCCCCCC>[CH2:1]([Si:9]([O:20][CH2:19][CH2:18][O:17][CH2:16][CH2:15][O:14][CH3:13])([O:20][CH2:19][CH2:18][O:17][CH2:16][CH2:15][O:14][CH3:13])[O:20][CH2:19][CH2:18][O:17][CH2:16][CH2:15][O:14][CH3:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 8134Diethylene Glycol Monomethyl EtherHCID 21354Octyltrichlorosilane

생성물 1

HCID 19427131HCID 19427131, 화합물

시약·촉매·용매 1

HCID 8900Heptane용매

반응 조건

온도
80 °C

실험 절차

To a dry flask fitted with an agitator, thermometer, additional funnel and reflux condenser was charged 222.8 g (0.90 mole) of octyltrichlorosilane and 225 g of heptane. The mixture was blanketed with nitrogen, heated to 80° C. and 333.7 g (2.78 mole) of 2-(2-methoxyethoxy)ethanol was added slowly over a 2 hour period. Hydrogen chloride was evolved from the mixture. After the addition was complete heating of the reaction was continued for 24 hours at 80° C. Then the solvent and all volatile components of the mixture were removed under vacuum, producing 451 g of the clear, colorless liquid product.

후처리

  1. customTo a dry flask fitted with an agitator
  2. temperaturethermometer, additional funnel and reflux condenser
  3. additionAfter the addition
  4. temperaturewas complete heating of the reaction
  5. customThen the solvent and all volatile components of the mixture were removed under vacuum
  6. customproducing 451 g of the clear, colorless liquid product

출처 및 근거

ORD 기록
ord-52c37a1263d54e1fabd252f7eb585341
출처 데이터셋
uspto-grants-1996_09
특허 번호
US05552476

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