Hydrochloric Acid → 3-benzyl-5,6,7,8-tetrahydro-1H-pyrido[4,3-d]pyrimidine-2,4-dione hydrochloride

HRID 742966노트

반응식

HRID 742966 반응식
[CH2:1]([N:8]1[C:13](=[O:14])[C:12]2[CH2:15][NH:16][CH2:17][CH2:18][C:11]=2[NH:10][C:9]1=[O:19])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[ClH:20]>O>[ClH:20].[CH2:1]([N:8]1[C:13](=[O:14])[C:12]2[CH2:15][NH:16][CH2:17][CH2:18][C:11]=2[NH:10][C:9]1=[O:19])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 194233353-benzyl-5,6,7,8-tetrahydro-1H-pyrido[4,3-d]pyrimidine-2,4-dione

생성물 1

HCID 194233343-benzyl-5,6,7,8-tetrahydro-1H-pyrido[4,3-d]pyrimidine-2,4-dione hydrochloride

시약·촉매·용매 1

HCID 962Water용매

실험 절차

9.4 g of 3-benzyl-5,6,7,8-tetrahydro-1H-pyrido[4,3-d]-pyrimidine-2,4-dione were suspended in 250 ml of water, the equivalent amount of 1 N HCl was added and the solution formed was filtered and concentrated under vacuum. 9.9 g of 3-benzyl-5,6,7,8-tetrahydro-1H-pyrido[4,3-d]pyrimidine-2,4-dione hydrochloride were obtained from the residue after purification by recrystallization from isopropanol.

후처리

  1. customthe solution formed
  2. filtrationwas filtered
  3. concentrationconcentrated under vacuum

출처 및 근거

ORD 기록
ord-53f30d7e9842416aaa5eed1bc740ce8f
출처 데이터셋
uspto-grants-1996_09
특허 번호
US05556854

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