Acetic Acid → Acetaldehyde, 2-[4-(1,1-dimethylethyl)phenoxy]-

HRID 743087

반응식

HRID 743087 반응식
[CH3:1][C:2]([C:5]1[CH:17]=[CH:16][C:8]([O:9][CH2:10][CH:11](OC)[O:12]C)=[CH:7][CH:6]=1)([CH3:4])[CH3:3].C(O)(=O)C.Cl>O>[CH3:4][C:2]([C:5]1[CH:6]=[CH:7][C:8]([O:9][CH2:10][CH:11]=[O:12])=[CH:16][CH:17]=1)([CH3:1])[CH3:3]

참가 물질

5

반응물 3

HCID 176Acetic AcidHCID 313Hydrochloric AcidHCID 3085718Benzene, 1-(2,2-dimethoxyethoxy)-4-(1,1-dimethylethyl)-

생성물 1

HCID 166373Acetaldehyde, 2-[4-(1,1-dimethylethyl)phenoxy]-

시약·촉매·용매 1

HCID 962Water용매

실험 절차

To a mixture of 5.00 g (0.021 mol.) of 2-[4-(1,1-dimethylethyl)phenoxy]-1,1-dimethoxyethane and 60 ml of acetic acid, there was added 6 ml of hydrochloric acid (36N) and the reaction mixture was stirred at room temperature for one hour. Then the reaction mixture was poured into 300 ml of cold water and filtrated quickly to recover a resultant white precipitate. The precipitate was obtained as a wet cake of 2-[4-(1,1-dimethylethyl) phenoxy]acetoaldehyde without being dried too much and was quickly used in the next step of the production procedure.

후처리

  1. filtrationfiltrated quickly
  2. customto recover a resultant white precipitate

출처 및 근거

ORD 기록
ord-08169f95fa504cdc803f5e48f99e6cc7
출처 데이터셋
uspto-grants-1996_09
특허 번호
US05556867

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