Iodoethane → 2-Propenoic acid, 3-(4-ethoxy-3-methoxyphenyl)-, ethyl ester, (E)-

반응식

[OH:1][C:2]1[CH:14]=[CH:13][C:5](/[CH:6]=[CH:7]/[C:8]([O:10][CH2:11][CH3:12])=[O:9])=[CH:4][C:3]=1[O:15][CH3:16].[CH2:17](I)[CH3:18]>>[CH2:17]([O:1][C:2]1[CH:14]=[CH:13][C:5](/[CH:6]=[CH:7]/[C:8]([O:10][CH2:11][CH3:12])=[O:9])=[CH:4][C:3]=1[O:15][CH3:16])[CH3:18]

참가 물질

반응물 2

HCID 6340Iodoethane

HCID 736681Ethyl Ferulate

생성물 1

HCID 53772382-Propenoic acid, 3-(4-ethoxy-3-methoxyphenyl)-, ethyl ester, (E)-수율 84.5%

실험 절차

Following a procedure similar to that described in Preparation 116, but using 5.83 g of ethyl (E)-4-hydroxy-3-methoxycinnamate and 5.61 g of ethyl iodide, 5.55 g of the title compound were obtained as a solid material.

후처리

customthat described in Preparation 116

출처 및 근거

ORD 기록: ord-d4a5d5bb98524116bcfb311e2d00b8af
출처 데이터셋: uspto-grants-1996_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05559109

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