반응식
[NH2:1][C:2]1[CH:3]=[CH:4][C:5]2[C:14]([CH:15]=1)=[N:13][C:12]([N:16]([CH2:19][CH3:20])[CH2:17][CH3:18])=[C:11]1[C:6]=2[CH:7]=[CH:8][C:9]([NH2:21])=[CH:10]1.[CH:22]([N:24]1[CH2:28][CH2:27][CH2:26][CH2:25]1)=O.[CH2:29]([N:31]([CH2:34][CH3:35])[CH:32]=O)[CH3:30]>>[CH2:17]([N:16]([CH2:19][CH3:20])[C:12]1[N:13]=[C:14]2[C:5](=[C:6]3[C:11]=1[CH:10]=[C:9]([N:21]=[CH:22][N:24]1[CH2:28][CH2:27][CH2:26][CH2:25]1)[CH:8]=[CH:7]3)[CH:4]=[CH:3][C:2]([N:1]=[CH:32][N:31]1[CH2:34][CH2:35][CH2:30][CH2:29]1)=[CH:15]2)[CH3:18]참가 물질
4
실험 절차
As in Example 14, but using 3,8-diamino-6-diethylaminophenanthridine and N-formylpyrrolidine instead of 3,8-diamino-6-dimethylaminophenanthridine and N,N-diethylformamide. Yield 66%, melting point 149°-150° C. (chloroform/petroleum ether (60°-80° C.)).
출처 및 근거
- ORD 기록
- ord-97ac297e36e14eefa5a32fef4f37b4e5
- 출처 데이터셋
- uspto-grants-1986_07
- 특허 번호
- US04599409
연결된 노트
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