Sodium borohydride → HCID 23310928, 화합물

반응식

[BH4-].[Na+].[C:3]([CH:6]1[CH2:10][CH2:9][CH:8]([CH3:11])[C:7]1([CH3:14])[CH:12]=[O:13])([CH3:5])=[CH2:4]>C(O)(C)C>[C:3]([CH:6]1[CH2:10][CH2:9][CH:8]([CH3:11])[C:7]1([CH3:14])[CH2:12][OH:13])([CH3:5])=[CH2:4]

참가 물질

실험 절차

Into a 250 ml flask equipped with stirrer, thermometer reflux condensor, heating mantle and nitrogen blanket apparatus are placed 15 grams of sodium borohydride, 100 ml anhydrous isopropyl alcohol and 65 grams of 2-isopropenyl-1,5-dimethylcyclopentane carboxaldehyde having the structure: ##STR26## prepared according to U.S. Pat. No. 4,474,992 issued on Oct. 2, 1984.

후처리

customInto a 250 ml flask equipped with stirrer
temperaturethermometer reflux condensor, heating mantle and nitrogen blanket apparatus
custom##STR26## prepared

출처 및 근거

ORD 기록: ord-bb0f43f23f4b4f94ab1524f8c3e67002
출처 데이터셋: uspto-grants-1986_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04601850

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참가 물질

반응물 2

HCID 4311764Sodium borohydride

HCID 233109291,2-Dimethyl-5-(prop-1-en-2-yl)cyclopentane-1-carbaldehyde

생성물 1

HCID 23310928HCID 23310928, 화합물

시약·촉매·용매 1

HCID 3776Isopropanol용매

실험 절차

후처리

customInto a 250 ml flask equipped with stirrer
temperaturethermometer reflux condensor, heating mantle and nitrogen blanket apparatus
custom##STR26## prepared

출처 및 근거

ORD 기록: ord-bb0f43f23f4b4f94ab1524f8c3e67002
출처 데이터셋: uspto-grants-1986_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04601850

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불러오는 중…