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llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
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Hydrochloric Acid → Acetate

HRID 745897
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HRID 745897 반응식
[CH3:1][O:2][C:3](=[O:9])[C@H:4]([C@@H:6]([CH3:8])[OH:7])[NH2:5].O.Cl>C(O)(=O)C>[CH3:1][O:2][C:3](=[O:9])[C@H:4]([C@@H:6]([CH3:8])[OH:7])[NH2:5].[C:3]([O-:9])(=[O:2])[CH3:4]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

6

반응물 3

HCID 313Hydrochloric AcidHCID 962WaterHCID 2734894Methyl threoninate

생성물 2

HCID 175Acetate수율 90.2%HCID 2734894Methyl threoninate

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

1.5 ml of a 5M solution of L-threonine methyl ester, acetate containing 200 mg of porcine insulin were prepared by dissolving 200 mg of porcine insulin in 750 μ liters of 10M acetic acid and adding 1 g of L-threonine methyl ester thereto. 2 mg of porcine trypsin were added, and the clear reaction mixture having a pH value of 6.3 was left at 20° C. The reaction was stopped after 90 hours by adding 15 ml of water and adjusting the pH value to 3 with 5N hydrochloric acid.

후처리

  1. addition2 mg of porcine trypsin were added
  2. waitwas left at 20° C

출처 및 근거

ORD 기록
ord-ad0c1e9526c24d0d9eae17aa01c053b2
출처 데이터셋
uspto-grants-1986_07
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04601979

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