Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl chloroformate → 1-Carbethoxy-3,5-dimethyl-4-piperidinone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl chloroformate | HCID 10928 | — |
| 반응물 | 1-Benzyl-3,5-dimethylpiperidin-4-one | HCID 22278920 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 1-Carbethoxy-3,5-dimethyl-4-piperidinone | HCID 22278887 | — |
반응 단계
Ethyl chloroformate (10.0 g, 90 mmol) was added to a stirred solution of 1-benzyl-3,5-dimethyl-4-piperidinone (5.0 g, 24 mmol) in benzene (20 ml), refluxed with stirring for 6 hr and concentrated to dryness to give 1-carbethoxy-3,5-dimethyl-4-piperidinone as oil. Yield 4.51 g (90%), C10H17NO3, m/z 200 (M+1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07393957B2 |
| 출처 데이터셋 | uspto-grants-2008_07 |
| ORD ID | ord-cd7a45ef50c14b30944e8455f01f9268 |
| 출처 메모 | uspto-grants-2008_07 |