Bis(cyclohexylammonium)sulfate → HCID 131726955, 화합물

HRID 747589

반응식

HRID 747589 반응식
[S:1]([O-:5])([O-:4])(=[O:3])=[O:2].[NH4+].[NH4+].S(O)(O)(=O)=[O:9].C1(N)CCCCC1.C1(N)CCCCC1.S(O)(O)(=O)=[O:28].[CH:32]1([NH:38][CH:39]2[CH2:44][CH2:43][CH2:42][CH2:41][CH2:40]2)[CH2:37][CH2:36][CH2:35][CH2:34][CH2:33]1.[CH:45]1([NH:51][CH:52]2[CH2:57][CH2:56][CH2:55][CH2:54][CH2:53]2)[CH2:50][CH2:49][CH2:48][CH2:47][CH2:46]1>>[S:1]([OH:5])([OH:4])(=[O:3])=[O:2].[CH:39]1([N:38]([CH:32]2[CH2:33][CH2:34][CH2:35][CH2:36][CH2:37]2)[OH:28])[CH2:40][CH2:41][CH2:42][CH2:43][CH2:44]1.[CH:52]1([N:51]([CH:45]2[CH2:46][CH2:47][CH2:48][CH2:49][CH2:50]2)[OH:9])[CH2:53][CH2:54][CH2:55][CH2:56][CH2:57]1

참가 물질

4

반응물 3

HCID 159837Bis(cyclohexylammonium)sulfateHCID 6097028Ammonium SulfateHCID 131726956HCID 131726956, 화합물

생성물 1

HCID 131726955HCID 131726955, 화합물

실험 절차

It can be seen from the NMR spectrum which is then measured that DCHAS has been formed. Traces of oxime, ammonium sulfate, CHAS, cyclohexylamine hemisulfate and dicyclohexylamine hemisulfate can be discerned as impurities in the NMR spectrum.

후처리

  1. customhas been formed

출처 및 근거

ORD 기록
ord-b2308dba9c2b4fe8aaa6de3fb1883cc3
출처 데이터셋
uspto-grants-2008_07
특허 번호
US07396959B2

연결된 노트

불러오는 중…