Triethylamine → HCID 62006965, 화합물

HRID 747687노트

반응식

HRID 747687 반응식
Cl[C:2]1[CH:7]=[CH:6][N:5]=[CH:4][CH:3]=1.[CH3:8][NH:9][CH2:10][C:11]([O:13][CH2:14][CH3:15])=[O:12].C(N(CC)CC)C.C(OCC)(=O)C>C1(C)C(C)=CC=CC=1>[CH3:8][N:9]([CH2:10][C:11]([O:13][CH2:14][CH3:15])=[O:12])[C:2]1[CH:7]=[CH:6][N:5]=[CH:4][CH:3]=1

참가 물질

6

반응물 4

HCID 8471TriethylamineHCID 8857Ethyl AcetateHCID 122884-ChloropyridineHCID 95849Glycine, N-methyl-, ethyl ester

생성물 1

HCID 62006965HCID 62006965, 화합물

시약·촉매·용매 1

HCID 7237O-Xylene용매

실험 절차

17 g (113 mmol) of 4-chloropyridine, 17 g (111 mmol) of ethyl (methylamino)acetate and 47 ml (333 mmol) of triethylamine were stirred in 350 ml of xylene at 130° C. for 24 hours. After the treatment with ethyl acetate as the extractant in an ordinary manner, the title compound was obtained.

출처 및 근거

ORD 기록
ord-81974470bfe646ada75627fef3aaac0e
출처 데이터셋
uspto-grants-2008_07
특허 번호
US07396844B1

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