Hydrochloric Acid → HCID 68833752, 화합물

HRID 747688노트

반응식

HRID 747688 반응식
[CH3:1][N:2]([CH2:9][C:10]([O:12]CC)=[O:11])[C:3]1[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=1.[ClH:15]>O1CCOCC1>[ClH:15].[CH3:1][N:2]([CH2:9][C:10]([OH:12])=[O:11])[C:3]1[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=1

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 62006965HCID 62006965, 화합물

생성물 1

HCID 68833752HCID 68833752, 화합물

시약·촉매·용매 1

HCID 312751,4-Dioxane용매

반응 조건

온도
95 °C

실험 절차

1.28 g (6.60 mmol) of ethyl [N-methyl-N-(pyridine-4-yl)amino]acetate was stirred in 30 ml of dioxane. 26 ml of 1 N hydrochloric acid was added to the resultant mixture, and they were stirred at 95° C. for 20 hours. The solvent was evaporated under reduced pressure to obtain the title compound.

후처리

  1. customThe solvent was evaporated under reduced pressure

출처 및 근거

ORD 기록
ord-d50aa3187b334e6f9906fff4cd7c8c1d
출처 데이터셋
uspto-grants-2008_07
특허 번호
US07396844B1

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