HCID 17788760, 화합물 → 3-(3-Cyanophenoxy)propanoic acid
반응식
[C:1]([C:3]1[CH:4]=[C:5]([CH:13]=[CH:14][CH:15]=1)[O:6][CH2:7][CH2:8][C:9]([O:11]C)=[O:10])#[N:2]>Cl>[C:1]([C:3]1[CH:4]=[C:5]([CH:13]=[CH:14][CH:15]=1)[O:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10])#[N:2]참가 물질
3
실험 절차
500 mg (2.4 mmol) of methyl 3-(3-cyanophenoxy)propionate was heated in 40 ml of 6 N hydrochloric acid at 70° C. for 30 minutes. After the extraction with ethyl acetate, the extract was washed with saturated aqueous NaCl solution and then dried on anhydrous magnesium sulfate. The solvent was evaporated to obtain the title compound.
후처리
- extractionAfter the extraction with ethyl acetate
- washthe extract was washed with saturated aqueous NaCl solution
- dry with materialdried on anhydrous magnesium sulfate
- customThe solvent was evaporated
출처 및 근거
- ORD 기록
- ord-a0f90bcfe61f4b89968b8c87665793a1
- 출처 데이터셋
- uspto-grants-2008_07
- 특허 번호
- US07396844B1
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