Ammonia → Caprolactam

HRID 78680

반응식

HRID 78680 반응식
C1(=[N:7]O)CCCCC1.[S:9](=[O:13])(=[O:12])([OH:11])[OH:10].OS(O)(=O)=O.O=S(=O)=O.S(O)(O)(=O)=O.[C:28]1(=[O:35])[NH:34][CH2:33][CH2:32][CH2:31][CH2:30][CH2:29]1.[NH3:36]>>[C:28]1(=[O:35])[NH:34][CH2:33][CH2:32][CH2:31][CH2:30][CH2:29]1.[S:9]([O-:13])([O-:12])(=[O:11])=[O:10].[NH4+:7].[NH4+:36]

참가 물질

7

실험 절차

The Beckmann rearrangement of the cyclohexanone oxime is carried out with sulfuric acid or oleum. The caprolactam sulfate prepared in this case and excess sulfuric acid are reacted with ammonia to give caprolactam and ammonium sulfate.

출처 및 근거

ORD 기록
ord-01f4839d1f2846ee93e0257eb0d561d9
출처 데이터셋
uspto-grants-2014_09
특허 번호
US08841445B2

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