Hydrochloric Acid → HCID 55285125, 화합물

반응식

C(OC(=O)[NH:7][C@@H:8]1[CH2:13][CH2:12][N:11]([CH3:14])[CH2:10][C@H:9]1[O:15][CH3:16])(C)(C)C.Cl>>[CH3:16][O:15][C@H:9]1[C@H:8]([NH2:7])[CH2:13][CH2:12][N:11]([CH3:14])[CH2:10]1

참가 물질

반응물 2

HCID 313Hydrochloric Acid

HCID 58522509HCID 58522509, 화합물

생성물 1

HCID 55285125HCID 55285125, 화합물

실험 절차

Tert-butyl((3R,4R)-3-methoxy-1-methyl-piperidin-4-yl)-carbamate (3.01 g) is combined with HCl (4 molar in dioxane, 25 mL). After 1 h the reaction mixture is freed from the solvent in vacuo and used in the next step without any further purification.

후처리

customused in the next step without any further purification

출처 및 근거

ORD 기록: ord-b1c6daa410044df38f2e64041c452c3a
출처 데이터셋: uspto-grants-2014_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08846689B2

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