Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cesium carbonate → HCID 70817494, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cesium carbonate | HCID 10796 | — |
| 반응물 | Methyl 2-bromopropionate | HCID 95576 | — |
| 반응물 | 2-(4-chlorophenyl)-N-[5-(7H-pyrrolo[2,3-d]pyrimidin-5-ylcarbonyl)pyridin-3-yl]acetamide | HCID 70817645 | — |
| 생성물 | HCID 70817494 | HCID 70817494 | — |
반응 단계
The title compound was prepared according to the method described for Example 229 using 2-(4-chlorophenyl)-N-[5-(7H-pyrrolo[2,3-d]pyrimidin-5-ylcarbonyl)pyridin-3-yl]acetamide (Example 308), methyl 2-bromopropionate and cesium carbonate. Purified using preparative HPLC (method 1) to afford the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08846698B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-9a4f5f942894436a8a41558eb19d246d |
| 출처 메모 | uspto-grants-2014_09 |