huagongshe.com
HRID82122

反应详情

EQUATION

反应方程式

HRID 82122 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[Cs+].[Cs+]
HCID10796

Cesium carbonate

CCs2O3

结构：COC(=O)C(C)Br
HCID95576

Propanoic acid, 2-bromo-, methyl ester

C4H7BrO2

结构：O=C(Cc1ccc(Cl)cc1)Nc1cncc(C(=O)c2c[nH]c3ncncc23)c1
HCID70817645

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)C(C)n1cc(C(=O)c2cncc(NC(=O)Cc3ccc(Cl)cc3)c2)c2cncnc21
HCID70817494

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to the method described for Example 229 using 2-(4-chlorophenyl)-N-[5-(7H-pyrrolo[2,3-d]pyrimidin-5-ylcarbonyl)pyridin-3-yl]acetamide (Example 308), methyl 2-bromopropionate and cesium carbonate. Purified using preparative HPLC (method 1) to afford the title compound.

WORKUP

后处理

  1. customThe title compound was prepared
  2. customPurified