Hydrochloric Acid → HCID 131730803, 화합물

HRID 83823

반응식

HRID 83823 반응식
[CH3:1][N:2]1[C:7]2=[N:8][CH2:9][CH2:10][CH2:11][N:6]2[CH2:5][CH2:4][CH2:3]1.[ClH:12]>CCOCC>[ClH:12].[CH3:1][N:2]1[C:7]2=[N:8][CH2:9][CH2:10][CH2:11][N:6]2[CH2:5][CH2:4][CH2:3]1

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 1235837-Methyl-1,5,7-triazabicyclo[4.4.0]dec-5-ene

생성물 1

HCID 131730803HCID 131730803, 화합물

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

A flame dried flask was charged with MTBD (0.25 g, 1.63 mmol), ether (10 mL) and a stirbar under dry nitrogen atmosphere. With vigorous stirring a 1M ethereal HCl solution (1.6 mL) was then added to form a white precipitate. Stirring was continued for 1 hour then excess solvent was decanted to yield 0.29 g (94%). The salt was then dried under high vacuum.

후처리

  1. customA flame dried flask
  2. additionwas then added
  3. customto form a white precipitate
  4. customexcess solvent was decanted
  5. customto yield 0.29 g (94%)
  6. customThe salt was then dried under high vacuum

출처 및 근거

ORD 기록
ord-e12c52601aad40bdbaaefe1cc77a32ec
출처 데이터셋
uspto-grants-2014_09
특허 번호
US08846851B2

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