Acridan → 10-(Isopropyliminomethyl)acridan
반응식
[CH:1]1[C:14]2[CH2:13][C:12]3[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=3)[NH:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[CH:15]([NH:18][CH:19]=O)([CH3:17])[CH3:16].P(Cl)(Cl)(Cl)=O>>[CH:15]([N:18]=[CH:19][N:6]1[C:7]2[C:12](=[CH:11][CH:10]=[CH:9][CH:8]=2)[CH2:13][C:14]2[CH:1]=[CH:2][CH:3]=[CH:4][C:5]1=2)([CH3:17])[CH3:16]참가 물질
4
실험 절차
Reaction of acridan, isopropylformamide and phosphorus oxychloride according to the procedure of Example 1 provides the free base 10-[(ISOPROPYLIMINO)METHYL]ACRIDAN, m.p. 149.5°-150.5° C. (corr.), from n-hexane.
출처 및 근거
- ORD 기록
- ord-8bd3c2db9e1c4c93b91a1a03c4d485d5
- 출처 데이터셋
- uspto-grants-1978_06
- 특허 번호
- US04094981
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