Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Desipramine Hydrochloride → Desipramine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Desipramine Hydrochloride | HCID 65327 | — |
| 용매 | Sodium Hydroxide | HCID 14798 | — |
| 생성물 | Desipramine | HCID 2995 | 99.1% |
반응 단계
To 6.02 g of desipramine hydrochloride was added 150 ml of 1N NaOH. The mixture was allowed to stir for 10 minutes. The aqueous mixture was extracted with 6×100 ml of chloroform. The combined chloroform layer was washed with 200 ml of water. The organic part was dried (Na2SO4) and concentrated to give 5.25 g of desipramine free base.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06368814B1 |
| 출처 데이터셋 | uspto-grants-2002_04 |
| ORD ID | ord-78cbff80e04c44a7a384b30c58aff007 |
| 출처 메모 | uspto-grants-2002_04 |