반응식
[OH-].[Na+].O[CH2:4][C:5]1[C:6]([CH2:11][OH:12])=[CH:7][CH:8]=[CH:9][CH:10]=1>>[CH2:11]1[O:12][CH2:4][C:5]2[C:6]1=[CH:7][CH:8]=[CH:9][CH:10]=2참가 물질
3
실험 절차
The procedure of Example 15 was performed except that the pH of the reaction mixture was regulated to 12 by use of sodium hydroxide. The reaction mixture was sampled for analysis. Formation of α,α′-dihydroxy-o-xylene was not observed. Instead, phthalan was formed at a yield of 96% based on α,α′-dichloro-o-xylene.
후처리
- aliquotThe reaction mixture was sampled for analysis
출처 및 근거
- ORD 기록
- ord-691be264de8b49cb99250fc961fc3048
- 출처 데이터셋
- uspto-grants-2002_04
- 특허 번호
- US06372921B1
연결된 노트
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