3-Fluorosalicylaldehyde → 2-Fluoro-6-(hydroxymethyl)phenol

HRID 843450노트

반응식

HRID 843450 반응식
[BH4-].[Na+].[F:3][C:4]1[C:5]([OH:12])=[C:6]([CH:9]=[CH:10][CH:11]=1)[CH:7]=[O:8]>>[F:3][C:4]1[CH:11]=[CH:10][CH:9]=[C:6]([CH2:7][OH:8])[C:5]=1[OH:12]

참가 물질

3

반응물 2

HCID 5877883-FluorosalicylaldehydeHCID 4311764Sodium borohydride

생성물 1

HCID 187554072-Fluoro-6-(hydroxymethyl)phenol

실험 절차

In an analogous manner to that described in (β) 3-fluoro-2-hydroxy-benzaldehyde was reduced by sodium borohydride to yield 2-fluoro-6-hydroxymethyl-phenol as a white solid; MS: 142 (M)+.

출처 및 근거

ORD 기록
ord-f03e6d1f7c12416e91c6357d8ec5d228
출처 데이터셋
uspto-grants-2002_04
특허 번호
US06376672B1

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