Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Bromo-6-methylbenzoic acid → N-[(2-bromo-6-methylphenyl)carbonyl]-4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Bromo-6-methylbenzoic acid | HCID 2735589 | — |
| 반응물 | 4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine methyl ester | HCID 69336975 | — |
| 생성물 | N-[(2-bromo-6-methylphenyl)carbonyl]-4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine | HCID 69335840 | — |
반응 단계
N-[(2-bromo-6-methylphenyl)carbonyl]-4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine was prepared from 4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine methyl ester and 2-bromo-6-methylbenzoic acid using the general procedures described in example 7 and was obtained as a white solid: mp 240-242° C. FAB-HRMS m/e calcd for C24H24BrN3O5 (M+H) 514.0978, found 514.0965.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06380387B1 |
| 출처 데이터셋 | uspto-grants-2002_04 |
| ORD ID | ord-905cf08e4be54333872800debcccb844 |
| 출처 메모 | uspto-grants-2002_04 |