Thiourea → HCID 178483278, 화합물

HRID 845402노트

반응식

HRID 845402 반응식
[ClH:1].Cl.[CH3:3][N:4]([CH2:6][C:7]1[CH:12]=[CH:11][N:10]=[C:9]([CH2:13][Cl:14])[CH:8]=1)[CH3:5].[NH2:15][C:16]([NH2:18])=[S:17]>C(O)C>[ClH:14].[ClH:1].[ClH:14].[CH3:3][N:4]([CH2:6][C:7]1[CH:12]=[CH:11][N:10]=[C:9]([CH2:13][NH:18][C:16](=[NH:15])[SH:17])[CH:8]=1)[CH3:5]

참가 물질

4

반응물 2

HCID 2723790ThioureaHCID 132926032-Chloromethyl-4-dimethylaminomethylpyridine dihydrochloride

생성물 1

HCID 178483278HCID 178483278, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

4-Dimethylaminomethyl-2-chloromethylpyridine dihydrochloride is reacted with thiourea in ethanol under reflux. Removal of the ethanol yields 4-dimethylaminomethyl-2-pyridylmethyl isothiourea trihydrochloride.

후처리

  1. temperatureunder reflux
  2. customRemoval of the ethanol

출처 및 근거

ORD 기록
ord-8a9126380a5c46d59de99e44f3b4a8c8
출처 데이터셋
uspto-grants-1988_07
특허 번호
US04758576

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