Sodium → HCID 20130574, 화합물

HRID 845912노트

반응식

HRID 845912 반응식
[Cl:1][C:2]1[CH:13]=[C:12]([F:14])[C:11]([NH:15][C:16]([NH:18][C:19]([CH2:26][CH3:27])=[CH:20][C:21](OCC)=[O:22])=[O:17])=[CH:10][C:3]=1[C:4]([O:6][CH:7]([CH3:9])[CH3:8])=[O:5].[Na]>C(O)(C)C>[Cl:1][C:2]1[CH:13]=[C:12]([F:14])[C:11]([N:15]2[C:21](=[O:22])[CH:20]=[C:19]([CH2:26][CH3:27])[NH:18][C:16]2=[O:17])=[CH:10][C:3]=1[C:4]([O:6][CH:7]([CH3:9])[CH3:8])=[O:5]

참가 물질

4

반응물 2

HCID 5360545SodiumHCID 53806823HCID 53806823, 화합물

생성물 1

HCID 20130574HCID 20130574, 화합물

시약·촉매·용매 1

HCID 3776Isopropanol용매

실험 절차

using isopropyl 2-chloro-4-fluoro-5-{3-[2-(ethoxycarbonyl)-1-ethylvinyl]ureido}-benzoate with sodium isopropylate in isopropanol there is obtained isopropyl 2-chloro-4-fluoro-5-[3,6-dihydro-4-ethyl-2,6-dioxo-1(2H)-pyrimidinyl]-benzoate, m.p. 121°-124° C.,

출처 및 근거

ORD 기록
ord-784e266fc33f4d5bac0973360ef8daf2
출처 데이터셋
uspto-grants-1988_07
특허 번호
US04760163

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