Methanol → HCID 13693406, 화합물

HRID 846236노트

반응식

HRID 846236 반응식
[CH3:1][S:2][C:3]1[CH:8]=[CH:7][C:6]([C:9](=[O:17])[CH:10]([CH3:16])[CH2:11][C:12]([O:14]C)=[O:13])=[CH:5][CH:4]=1.[OH-].[Na+].CO>C1COCC1>[CH3:1][S:2][C:3]1[CH:4]=[CH:5][C:6]([C:9](=[O:17])[CH:10]([CH3:16])[CH2:11][C:12]([OH:14])=[O:13])=[CH:7][CH:8]=1

참가 물질

5

반응물 3

HCID 887MethanolHCID 14798Sodium HydroxideHCID 13693403HCID 13693403, 화합물

생성물 1

HCID 13693406HCID 13693406, 화합물

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

The ester from Step B (1.07 g) was saponified with 1N NaOH (5 ml) and methanol (5 ml) and THF (5 ml) to provide after acidification, extraction into CH and evaporation to dryness the title compound, mp 69°-71° C.

후처리

  1. customto provide
  2. extractionafter acidification, extraction
  3. custominto CH and evaporation to dryness the title compound, mp 69°-71° C.

출처 및 근거

ORD 기록
ord-6efb5349747849ec9cd47f01c1840f87
출처 데이터셋
uspto-grants-1992_08
특허 번호
US05135940

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