Water → HCID 16790146, 화합물
반응식
O.[OH-].[Na+].Cl.[Cl:5][C:6]1[CH:7]=[C:8]([CH:10]=[CH:11][C:12]=1[O:13][CH2:14][CH2:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)[NH2:9]>C(O)C>[Cl:5][C:6]1[CH:7]=[C:8]([CH:10]=[CH:11][C:12]=1[O:13][CH2:14][CH2:15][C:16]1[CH:17]=[CH:18][CH:19]=[CH:20][CH:21]=1)[NH2:9]참가 물질
5
실험 절차
To a mixture of water (50 ml), ethanol (50 ml) and 50% aqueous sodium hydroxide (25 ml) is added 3-chloro-4-(phenethyloxy)aniline hydrochloride (8.25 g; 0.0290 mol). When the solid is all dissolved, the solution is extracted with ether (3×100 ml). The ether solution is washed with brine, dried over potassium carbonate and concentrated under vacuum to yield 5.16 g (77%) of a tan oil. This oil is distilled at 140° C. under 0.005 ml vacuum to afford the product, a colorless liquid.
후처리
- extractionthe solution is extracted with ether (3×100 ml)
- washThe ether solution is washed with brine
- dry with materialdried over potassium carbonate
- concentrationconcentrated under vacuum
출처 및 근거
- ORD 기록
- ord-ba747bf6921f452da748698f0b95c17e
- 출처 데이터셋
- uspto-grants-1981_10
- 특허 번호
- US04294986
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