HCID 70577148, 화합물 → HCID 70577147, 화합물

HRID 848482노트

반응식

HRID 848482 반응식
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[C:17]3[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=3)[N:11]=[C:10]([NH:18][CH2:19][CH2:20][N:21]([CH2:24][CH3:25])[CH2:22][CH3:23])[C:9]2=[O:26])=[CH:4][CH:3]=1>C(Cl)(Cl)Cl>[ClH:1].[ClH:1].[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[C:17]3[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=3)[N:11]=[C:10]([NH:18][CH2:19][CH2:20][N:21]([CH2:24][CH3:25])[CH2:22][CH3:23])[C:9]2=[O:26])=[CH:4][CH:3]=1

참가 물질

3

반응물 1

HCID 70577148HCID 70577148, 화합물

생성물 1

HCID 70577147HCID 70577147, 화합물

시약·촉매·용매 1

HCID 6212Chloroform용매

실험 절차

1-(4-Chlorophenyl)-1,2-dihydro-3-(N,N-diethylamino)ethylaminoquinoxalin-2-one (5.0 g) was dissolved in chloroform (150 ml) and dry hydrogen chloride was bubbled through the solution for 10 minutes. The precipitate was dried and recrystallised from ethanol giving the title compound mp >240° C.

후처리

  1. customdry hydrogen chloride was bubbled through the solution for 10 minutes
  2. customThe precipitate was dried
  3. customrecrystallised from ethanol giving the title compound mp >240° C.

출처 및 근거

ORD 기록
ord-a21151614f2b40ed92f2eff4c8947795
출처 데이터셋
uspto-grants-1981_10
특허 번호
US04296114

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