Hydrochloric Acid → HCID 67167889, 화합물
반응식
[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4](/[CH:8]=[CH:9]/[N+:10]([O-:12])=[O:11])[C:3]=1[O:13]COC.Cl>CO.O1CCOCC1>[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4](/[CH:8]=[CH:9]/[N+:10]([O-:12])=[O:11])[C:3]=1[OH:13]참가 물질
5
실험 절차
To a suspension of Example 383B in methanol (15 mL) was added 4 N HCl in dioxane (1 mL). The mixture was stirred for 4 hours, concentrated, and diluted with water. The precipitates were collected to afford the titled compound.
후처리
- concentrationconcentrated
- additiondiluted with water
- customThe precipitates were collected
출처 및 근거
- ORD 기록
- ord-eda001caede046d5b5e12f4a20bc9b01
- 출처 데이터셋
- uspto-grants-2014_09
- 특허 번호
- US08846951B2
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