Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Sulfite → 2-(Butylsulfonyl)cyclopentanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Sulfite | HCID 24437 | — |
| 반응물 | Monoperoxyphthalic acid | HCID 75329 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 2-(Butylsulfonyl)cyclopentanone | HCID 289555 | — |
반응 단계
2-Buthylthiocyclopentanone (88 g) was reacted with a 30% excess solution of mono-perphthalic acid in ether at 0° C. After the reaction was completed, the excess mono-perphthalic acid was treated with sodium sulfite, and the resultant solution was washed, evaporated to remove the solvent, and then distilled, thereby giving 2-butylsulfonylcyclopentanone (78 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07252849B2 |
| 출처 데이터셋 | uspto-grants-2007_08 |
| ORD ID | ord-e82c9b732d564f92a08e72aaa22da92b |
| 출처 메모 | uspto-grants-2007_08 |