HRID851835

反应详情

EQUATION

反应方程式

HRID 851835 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

2-Buthylthiocyclopentanone (88 g) was reacted with a 30% excess solution of mono-perphthalic acid in ether at 0° C. After the reaction was completed, the excess mono-perphthalic acid was treated with sodium sulfite, and the resultant solution was washed, evaporated to remove the solvent, and then distilled, thereby giving 2-butylsulfonylcyclopentanone (78 g).

WORKUP

后处理

  1. washthe resultant solution was washed
  2. customevaporated
  3. customto remove the solvent
  4. distillationdistilled