Dimethylformamide dimethyl acetal → HCID 72466434, 화합물

HRID 852439노트

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HRID 852439 반응식
[NH:1]([C:5]1[CH:6]=[C:7]([S:11]([NH2:14])(=[O:13])=[O:12])[CH:8]=[CH:9][CH:10]=1)[C:2]([NH2:4])=[S:3].CO[CH:17](OC)[N:18]([CH3:20])[CH3:19]>>[CH3:17][N:18]([CH:20]=[N:14][S:11]([C:7]1[CH:8]=[CH:9][CH:10]=[C:5]([NH:1][C:2]([N:4]=[CH:17][N:18]([CH3:20])[CH3:19])=[S:3])[CH:6]=1)(=[O:12])=[O:13])[CH3:19]

참가 물질

3

반응물 2

HCID 78373Dimethylformamide dimethyl acetalHCID 431489173-Thioureido-benzenesulfonamide

생성물 1

HCID 72466434HCID 72466434, 화합물수율 82%

실험 절차

A mixture of 2.3 g (9.9 mmol) 3-Thioureido-benzenesulfonamide and 17 ml N,N-Dimethylformamide dimethyl acetal was heated for 2 h to 90° C. The precipitate was filtered of washed with DCM/diethyl ether 1:3 and dried to yield 2.8 g (82%) of the title compound.

후처리

  1. temperaturewas heated for 2 h to 90° C
  2. filtrationThe precipitate was filtered
  3. washof washed with DCM/diethyl ether 1:3
  4. customdried

출처 및 근거

ORD 기록
ord-4452ed59d260418a942b5ff2ee2dd0e4
출처 데이터셋
uspto-grants-2007_08
특허 번호
US07253197B2

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