Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → Perfluorooctanoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Octanoyl fluoride, 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro- | HCID 67634 | — |
| 생성물 | Perfluorooctanoic acid | HCID 9554 | — |
반응 단계
A 250 ml PFA vessel equipped with a stirrer was used. Water (100 g, 5.6 mol) was temperature conditioned to 60° C. within the vessel, following which C7F15COF (50 g, 0.120 mol; prepared by the method described in JP-A 8-231462) having a purity of 99.9 wt % was added dropwise under stirring in an attempt to form C7F15COOH by a hydrolysis reaction. However, a gel formed, which made stirring impossible.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07253315B2 |
| 출처 데이터셋 | uspto-grants-2007_08 |
| ORD ID | ord-ac8e42cdc53a4f5d8e452e14a54cd255 |
| 출처 메모 | uspto-grants-2007_08 |