反应详情

A 250 ml PFA vessel equipped with a stirrer was used. Water (100 g, 5.6 mol) was temperature conditioned to 60° C. within the vessel, following which C7F15COF (50 g, 0.120 mol; prepared by the method described in JP-A 8-231462) having a purity of 99.9 wt % was added dropwise under stirring in an attempt to form C7F15COOH by a hydrolysis reaction. However, a gel formed, which made stirring impossible.

1. customA 250 ml PFA vessel equipped with a stirrer
2. customconditioned to 60° C. within the vessel
3. customprepared by the method
4. additionwas added dropwise