HCID 21867058, 화합물 → 6-[4-(3-Aminophenyl)butoxy]hexyl acetate
반응식
[C:1]([O:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][O:11][CH2:12][CH2:13][C:14]#[C:15][C:16]1[CH:21]=[CH:20][CH:19]=[C:18]([N+:22]([O-])=O)[CH:17]=1)(=[O:3])[CH3:2]>CCO.O=[Pt]=O>[C:1]([O:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][O:11][CH2:12][CH2:13][CH2:14][CH2:15][C:16]1[CH:21]=[CH:20][CH:19]=[C:18]([NH2:22])[CH:17]=1)(=[O:3])[CH3:2]참가 물질
4
실험 절차
6-{[4-(3-Nitrophenyl)but-3-ynyl]oxy}hexyl acetate (2.973 g) was hydrogenated over PtO2 (300 mg) in EtOH over 1 h. The catalyst was removed by filtration and washed with EtOH. The combined filtrate and washings were concentrated under reduced pressure to give the title compound (2.844 g) LCMS RT=3.30 min.
후처리
- customThe catalyst was removed by filtration
- washwashed with EtOH
- concentrationThe combined filtrate and washings were concentrated under reduced pressure
출처 및 근거
- ORD 기록
- ord-86418d09047148dd989cadad2369ca55
- 출처 데이터셋
- uspto-grants-2006_12
- 특허 번호
- US07144908B2
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