Phthalic Anhydride → N,N-Dibutylformamide

HRID 860921노트

반응식

HRID 860921 반응식
C(Cl)(=O)C1C(=CC=CC=1)C(Cl)=O.C1(=O)OC(=O)C2=CC=CC=C12.[CH2:24]([N:28]([CH2:32][CH2:33][CH2:34][CH3:35])[C:29](Cl)=[O:30])[CH2:25][CH2:26][CH3:27]>>[CH2:24]([N:28]([CH2:32][CH2:33][CH2:34][CH3:35])[CH:29]=[O:30])[CH2:25][CH2:26][CH3:27]

참가 물질

4

반응물 3

HCID 6811Phthalic AnhydrideHCID 6955Phthaloyl chlorideHCID 83371Dibutylcarbamoyl chloride

생성물 1

HCID 12975N,N-Dibutylformamide

실험 절차

The crude product remains as a dark oil. According to HPLC analysis, it contains 83.8% by weight of phthaloyl chloride, 2.4% by weight of phthalic anhydride, and, according to GC analysis, 0.9 area % of N,N-dibutylcarbamoyl chloride. Based on the product, this corresponds to a crude yield of 97.8% of theory.

출처 및 근거

ORD 기록
ord-c40172eda5a949b1acf88fddb69d4519
출처 데이터셋
uspto-grants-2006_12
특허 번호
US07154003B2

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