Acetic Anhydride → 1-acetoxy-2-[2-(N,N-dimethylamino)ethoxy]-1-(1-naphthyl)ethane

HRID 862538노트

반응식

HRID 862538 반응식
Cl.[CH3:2][N:3]([CH2:5][CH2:6][O:7][CH2:8][CH:9]([C:11]1[C:20]2[C:15](=[CH:16][CH:17]=[CH:18][CH:19]=2)[CH:14]=[CH:13][CH:12]=1)[OH:10])[CH3:4].[C:21](OC(=O)C)(=[O:23])[CH3:22].C(N(CC)CC)C>N1C=CC=CC=1>[C:21]([O:10][CH:9]([C:11]1[C:20]2[C:15](=[CH:16][CH:17]=[CH:18][CH:19]=2)[CH:14]=[CH:13][CH:12]=1)[CH2:8][O:7][CH2:6][CH2:5][N:3]([CH3:2])[CH3:4])(=[O:23])[CH3:22]

참가 물질

5

반응물 3

HCID 7918Acetic AnhydrideHCID 8471TriethylamineHCID 675980182-[2-(N,N-dimethylamino)ethoxy]-1-(1-naphthyl)ethanol hydrochloride

생성물 1

HCID 540332121-acetoxy-2-[2-(N,N-dimethylamino)ethoxy]-1-(1-naphthyl)ethane

시약·촉매·용매 1

HCID 1049Pyridine용매

실험 절차

2-[2-(N,N-dimethylamino)ethoxy]-1-(1-naphthyl)ethanol hydrochloride was reacted with acetic anhydride in pyridine in the presence of triethylamine to obtain oily 1-acetoxy-2-[2-(N,N-dimethyl-amino)ethoxy]-1-(1-naphthyl)ethane (compound No. 300).

출처 및 근거

ORD 기록
ord-0ca6c8ea0e594a2ab82fb1d60ee1c6ed
출처 데이터셋
uspto-grants-1998_02
특허 번호
US05719150

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