Chloroform → HCID 2797868, 화합물
반응식
[N:1]1[CH:6]=[CH:5][C:4]([CH:7](O)[C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[CH:3][CH:2]=1.C(Cl)(Cl)[Cl:16].O=S(Cl)[Cl:21]>C(Cl)Cl>[ClH:16].[N:1]1[CH:6]=[CH:5][C:4]([CH:7]([Cl:21])[C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[CH:3][CH:2]=1참가 물질
5
실험 절차
To a solution of 27.75 g (0.15 mol) of (4-pyridyl)benzyl alcohol and 200 ml of chloroform is run in dropwise, at room temperature, a solution of 15.25 ml (0.2 mol) of SOCl2 and 50 ml of CH2Cl2.
후처리
- customat room temperature
출처 및 근거
- ORD 기록
- ord-d10fc50f700d493ab1ed685d939c5f84
- 출처 데이터셋
- uspto-grants-1998_02
- 특허 번호
- US05719168
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