Sodium borohydride → Benzenemethanol, 2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-
반응식
[Si:1]([O:8][C:9]1[CH:16]=[CH:15][CH:14]=[CH:13][C:10]=1[CH:11]=[O:12])([C:4]([CH3:7])([CH3:6])[CH3:5])([CH3:3])[CH3:2].[BH4-].[Na+]>CO>[Si:1]([O:8][C:9]1[CH:16]=[CH:15][CH:14]=[CH:13][C:10]=1[CH2:11][OH:12])([C:4]([CH3:7])([CH3:6])[CH3:5])([CH3:3])[CH3:2]참가 물질
4
실험 절차
A solution of 28 (200 mg) in methanol (5.5 ml) containing NaBH4 (28 mg) is stirred for 1 hour at room temperature. 29 (140 mg, 68%) is obtained after hydrolysis and customary extraction.
출처 및 근거
- ORD 기록
- ord-cface378f1e0442cb06387305829639a
- 출처 데이터셋
- uspto-grants-1996_10
- 특허 번호
- US05561119
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