Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl iodide → Methyl 2-amino-6-chlorobenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | 2-Amino-6-chlorobenzoic acid | HCID 75071 | — |
| 생성물 | Methyl 2-amino-6-chlorobenzoate | HCID 592849 | 78.4% |
반응 단계
Using the procedure described above in Preparation 1, 5.0 g (0.029 mol) of 6-chloroanthranilic acid and 2.75 ml (0.044 mol) of iodomethane were reacted in the presence of 4.08 g (0.073 mol) of powdered potassium hydroxide to give 4.22 g (78%) of methyl 6-chloroanthranilate as an oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05563163 |
| 출처 데이터셋 | uspto-grants-1996_10 |
| ORD ID | ord-8cd00d734c5444f1804c2288e1aabf23 |
| 출처 메모 | uspto-grants-1996_10 |