Methyl iodide → trans-3-(3-(2-Hexenyloxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide

HRID 865169노트

반응식

HRID 865169 반응식
[CH3:1][I:2].[CH2:3]([O:9][C:10]1[C:14]([C:15]2[CH:16]=[N:17][CH:18]=[CH:19][CH:20]=2)=[N:13][S:12][N:11]=1)/[CH:4]=[CH:5]/[CH2:6][CH2:7][CH3:8]>CC(C)=O>[I-:2].[CH2:3]([O:9][C:10]1[C:14]([C:15]2[CH:16]=[N+:17]([CH3:1])[CH:18]=[CH:19][CH:20]=2)=[N:13][S:12][N:11]=1)/[CH:4]=[CH:5]/[CH2:6][CH2:7][CH3:8]

참가 물질

4

반응물 2

HCID 6328Methyl iodideHCID 19075257trans-3-(3-(2-Hexenyloxy)-1,2,5-thiadiazol-4-yl)pyridine

생성물 1

HCID 19075386trans-3-(3-(2-Hexenyloxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

A mixture of methyl iodide (0.5 ml, 7.5 mmol) and trans-3-(3-(2-hexenyloxy)-1,2,5-thiadiazol-4-yl)pyridine (3 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 1.09 g (90%).

후처리

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 1.09 g (90%)

출처 및 근거

ORD 기록
ord-5c170fbf7c3249b78bd82db2251ebafb
출처 데이터셋
uspto-grants-1996_10
특허 번호
US05565475

반응 노트

불러오는 중…