4-Chlorophenyl Isocyanate → N-[[(4-chlorophenyl) amino]-carbonyl]-4-(4-morpholinyl) benzenesulfonamide

HRID 865316노트

반응식

HRID 865316 반응식
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]=[C:9]=[O:10])=[CH:4][CH:3]=1.[N:11]1([C:17]2[CH:22]=[CH:21][C:20]([S:23]([NH2:26])(=[O:25])=[O:24])=[CH:19][CH:18]=2)[CH2:16][CH2:15][O:14][CH2:13][CH2:12]1>CC(C)=O>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9]([NH:26][S:23]([C:20]2[CH:19]=[CH:18][C:17]([N:11]3[CH2:16][CH2:15][O:14][CH2:13][CH2:12]3)=[CH:22][CH:21]=2)(=[O:24])=[O:25])=[O:10])=[CH:4][CH:3]=1

참가 물질

4

반응물 2

HCID 76934-Chlorophenyl IsocyanateHCID 7354354-(Morpholin-4-yl)benzene-1-sulfonamide

생성물 1

HCID 15345719N-[[(4-chlorophenyl) amino]-carbonyl]-4-(4-morpholinyl) benzenesulfonamide

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

4-Chlorophenylisocyanate (2.61 g, 17 moles) was dissolved in 16 ml of acetone and was then added dropwise to the sulfonamide solution. The mixture was then stirred overnight at room temperature, resulting in the formation of a white solid.

후처리

  1. customresulting in the formation of a white solid

출처 및 근거

ORD 기록
ord-fdccf3362d874d0bba3eb0d86506ba63
출처 데이터셋
uspto-grants-1996_10
특허 번호
US05565494

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