Ethyl 4-amino-1-piperidinecarboxylate → HCID 23374509, 화합물

HRID 865647

반응식

HRID 865647 반응식
[NH2:1][CH:2]1[CH2:7][CH2:6][N:5]([C:8]([O:10][CH2:11][CH3:12])=[O:9])[CH2:4][CH2:3]1.C(O[C:16]1[CH:21]=[CH:20][N:19]=[CH:18][C:17]=1[N+:22]([O-:24])=[O:23])C>CC#N>[N+:22]([C:17]1[CH:18]=[N:19][CH:20]=[CH:21][C:16]=1[NH:1][CH:2]1[CH2:3][CH2:4][N:5]([C:8]([O:10][CH2:11][CH3:12])=[O:9])[CH2:6][CH2:7]1)([O-:24])=[O:23]

참가 물질

4

반응물 2

HCID 100867Ethyl 4-amino-1-piperidinecarboxylateHCID 3563054-Ethoxy-3-nitropyridine

생성물 1

HCID 23374509HCID 23374509, 화합물

시약·촉매·용매 1

HCID 6342Acetonitrile용매

실험 절차

A mixture of ethyl 4-amino-1-piperidinecarboxylate (3.53 g, 20.5 mmol) and 4-ethoxy-3-nitropyridine (3.65 g, 21/7 mmol) in CH3CN (25 mL) was heated at reflux for 40 hours. The reaction mixture was cooled to ambient temperature and concentrated in vacuo to give an orange syrup which was used without further purification.

후처리

  1. temperaturewas heated
  2. temperatureat reflux for 40 hours
  3. concentrationconcentrated in vacuo
  4. customto give an orange syrup which
  5. customwas used without further purification

출처 및 근거

ORD 기록
ord-5b8ae9819dc8446a9b95b612a6523f32
출처 데이터셋
uspto-grants-1996_10
특허 번호
US05567711

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