Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl 4-amino-1-piperidinecarboxylate → HCID 23374509, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl 4-amino-1-piperidinecarboxylate | HCID 100867 | — |
| 반응물 | 4-Ethoxy-3-nitropyridine | HCID 356305 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | HCID 23374509 | HCID 23374509 | — |
반응 단계
A mixture of ethyl 4-amino-1-piperidinecarboxylate (3.53 g, 20.5 mmol) and 4-ethoxy-3-nitropyridine (3.65 g, 21/7 mmol) in CH3CN (25 mL) was heated at reflux for 40 hours. The reaction mixture was cooled to ambient temperature and concentrated in vacuo to give an orange syrup which was used without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05567711 |
| 출처 데이터셋 | uspto-grants-1996_10 |
| ORD ID | ord-5b8ae9819dc8446a9b95b612a6523f32 |
| 출처 메모 | uspto-grants-1996_10 |