Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phosphorus sulfide (P2S5) → n-C8H17SP(S)Cl2
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phosphorus sulfide (P2S5) | HCID 14817 | — |
| 반응물 | Thiophosphoryl chloride | HCID 19883 | — |
| 반응물 | Dioctyl sulfide | HCID 75901 | — |
| 생성물 | n-C8H17SP(S)Cl2 | HCID 15833785 | 97.4% |
반응 단계
Following the procedure of the preceding Examples, 64.5 grams (0.25 mole) of (n-C8H17)2S, 18.5 grams (0.0416 mole) of P4S10 and 90 grams (0.53 mole) of PSCl3 were reacted at 190° C for 10 hours. The crude reaction mixture was distilled twice to provide 68 grams (49% yield) of n-C8H17SP(S)Cl2 having the following properties:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04100230 |
| 출처 데이터셋 | uspto-grants-1978_07 |
| ORD ID | ord-805d356ce5f6455fb182c447d55fbec9 |
| 출처 메모 | uspto-grants-1978_07 |