Sodium Hydroxide → inositol 1,2,6-triphosphate

HRID 867855

반응식

HRID 867855 반응식
[CH:1]1([O:32][P:33]([O-:36])([O-:35])=[O:34])[CH:6]([O:7][P:8]([O-:11])([O-:10])=[O:9])[CH:5]([O:12][P:13]([O-:16])([O-:15])=[O:14])[CH:4]([O:17]P([O-])([O-])=O)[CH:3]([O:22]P([O-])([O-])=O)[CH:2]1[O:27]P([O-])([O-])=O.[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[OH-].[Na+]>C(O)C>[C@H:4]1([OH:17])[CH:3]([OH:22])[C@@H:2]([OH:27])[C@@H:1]([O:32][P:33]([OH:36])([OH:35])=[O:34])[CH:6]([O:7][P:8]([OH:10])([OH:11])=[O:9])[C@@H:5]1[O:12][P:13]([OH:15])([OH:16])=[O:14]

참가 물질

4

반응물 2

HCID 14798Sodium HydroxideHCID 66391Phytate Persodium

생성물 1

HCID 65762inositol 1,2,6-triphosphate

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

100 ml of the fraction containing D-myo-inositol-1.2.6-triphosphate obtained in Example 15 was neutralized to a pH of about 7 with an aqueous solution of NaOH. After addition of 100 ml ethanol the volume of the solution was reduced by evaporation and the sodiumsalt was precipitated, centrifuged, recrystallized and dried in vacuum. The purified sodiumsalt of D-myo-inositol-1.2.6-triphosphate obtained was structurally confirmed by analysis with H-NMR.

후처리

  1. customwas reduced by evaporation
  2. customthe sodiumsalt was precipitated
  3. customrecrystallized
  4. customdried in vacuum

출처 및 근거

ORD 기록
ord-9f33052edcde4fbab35e0f7266edce33
출처 데이터셋
uspto-grants-1988_10
특허 번호
US04777134

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