HCID 14329809, 화합물 → 2-((E)-4-methoxybenzylidene)butan-1-al

HRID 868226노트

반응식

HRID 868226 반응식
[CH3:1][O:2][C:3]1[CH:14]=[CH:13][C:6](/[CH:7]=[C:8](\[CH2:11][CH3:12])/[CH2:9][OH:10])=[CH:5][CH:4]=1>C(Cl)(Cl)Cl.[O-2].[O-2].[Mn+4]>[CH3:1][O:2][C:3]1[CH:14]=[CH:13][C:6](/[CH:7]=[C:8](\[CH2:11][CH3:12])/[CH:9]=[O:10])=[CH:5][CH:4]=1

참가 물질

4

반응물 1

HCID 14329809HCID 14329809, 화합물

생성물 1

HCID 136347482-((E)-4-methoxybenzylidene)butan-1-al수율 73.1%

시약·촉매·용매 2

HCID 178418406HCID 178418406, 화합물촉매HCID 6212Chloroform용매

실험 절차

A mixture of 2-((E)-4-methoxybenzylidene)butan-1-ol (13 g) and manganese dioxide (130 g) in chloroform (600 ml) was stirred at room temperature for 20 hours. Manganese dioxide was filtered off by filtration and the filtrate was condensed to give 2-((E)-4-methoxybenzylidene)butan-1-al (9.4 g).

후처리

  1. filtrationManganese dioxide was filtered off by filtration
  2. customcondensed

출처 및 근거

ORD 기록
ord-736b5dd48b40411f95abbd4547a09c62
출처 데이터셋
uspto-grants-1988_10
특허 번호
US04778804

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